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3.6. The 3 H nucleus is more sensitive (1.21:1.00) for NMR measurements than is the proton. It also has a spin of 1/2, which is considered ideal for NMR measurements. Why is 3 H NMR not commonly used 3.7. Make tables or charts of the 29 Si and 31 P NMR shifts given in Section 4.3.1. Using your tabulations and your knowledge of chemical trends, suggest reasons for the trends that you observe. 3.8. Sketch the repeating units of the uranyl carboxylate polymers discussed in Section 3.4.1 verifying the seven-coordination suggested by the text. 3.9. Note that the symmetry variation in EPR g values is logical from the symmetry of the sites. That is, an isotropic site where x D y D z leads to gx D gy D gz or a single g value. Similarly an axial site where x D y 6D z leads to gx D gy 6D gz or g and gjj , respectively. An asymmetric site, where x 6D y 6D z leads to gx 6D gy 6D gz or g1 , g2 , and g3 . Using a set of character tables, determine the point groups that lead to isotropic, axial, and asymmetric g values. 3.10. Compare the relative o values in the two columns of Table 3.8 for ligands that are saturated donors, unsaturated donors, only donors, and acceptors. Explain any differences you note for one group versus another. Note: A lack of a trend for some ligands may be to the result of Jorgensen having primarily d6 species when he determined his general f values. 3.11. It has been shown fArcher; Bonds; Pribush, Inorg. Chem., 1972, 11, 1550g that tungsten(V) coordination compounds analogous to the polymer molecules exhibit ligand-to-metal charge-transfer transitions [whereas the tungsten(IV) species were previously shown to exhibit metal-to-ligand transitions]. If a local excess of the dione in the tungsten polymer synthesis caused some of the tungsten to be oxidized to tungsten(V), suggest an alternate interpretation for the broad low-energy spectrum of the insoluble polymer of tungsten noted in Section 3.4.3.
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The 1-D FT of p u denoted by P f is equal to the central slice at angle y of the 2-D FT of g x; y denoted by G fx ; fy : P f G f cos y; f sin y 18:3-1
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Obviously mechanical trading systems can be developed based on any number of objective criteria including interest rate differentials, gross domestic product, or earnings per share. Although this book in no way negates the validity of such fundamental tools in system development,9 I do argue that an inherent limitation in using such tools is that they require an indepth understanding of a particular market or trading instrument. By contrast, mathematical technical indicators do not require any particular specialized knowledge of the underlying fundamentals affecting a particular market on the part of system developers. This absence of expertise thereby allows traders to apply their system as readily to Asian equities or live cattle, soybeans or foreign exchange, sugar or natural gas. Although obvious benefits gained by participating in diverse markets will be examined in detail later, for now let me suggest that diversification into various low to negatively correlated asset classes increases the likelihood of improved rates of return on investment and often reduces the severity of peakto-valley drawdowns in equity.10
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Figure 19.3. The output of a 16-channel PHASAR at a center wavelength of 1.550 m, and channel spacing of 0.8 m [Lu, Ersoy].
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Part III: Healthy Eating: Natural, Nutritious Recipes
6.1.1. Area Formula
Component View
This loaf tastes great but takes an hour to bake, so plan ahead. If you won t eat the whole loaf within a few days, cut it in two and freeze half for another time. Preparation Time: 20 minutes Cooking Time: 60 minutes Yield: 1 loaf (12 slices)
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