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Figure 4.2.19 X-ray uorescence spectra for a stainless steel sample excited with a 244 Cm X-ray source, using a photomultiplier based GPSC and (a) 11 mm and (b) 25 mm diameter window collimations (Figure 8 of dos Santos et al.46 ). Reproduced by permission of The Institute of Electrical and Electronics Engineers, Inc. 2.5 14: Assembly Configurations and Display States
The term dimensional reduction refers to the process of dismantling the extended metal anion (M X) framework of a parent compound MXa upon reaction with an ionic reagent AbX, to form a new compound AnbMXa+n.16 The A cations, which are more electropositive than the metal (M), do not form strong covalent bonds with the X anions and, therefore, may be treated as lying outside the M X framework. The introduced X ions (for this chapter, X = S, Se, or Te) terminate connections between metal centers in the structure, yielding a less tightly connected or lower dimensional framework, which may locally retain aspects of the characteristic metal coordination and polyhedron connectivity of the original parent structure. For each additional AbX unit added to the parent structure (denoted by n ), additional M X M metal bond linkages are broken and the effective dimensionality of the MXa+n framework is progressively reduced (Fig. 3.1). As an example, a series of compounds develop from the interaction between SnSe2 and K2Se, including K4Sn3Se8 (n = 2/3),17 K2SnSe3 (n = 1),18 K6Sn2Se7 (n = 1.5),19 and K4SnSe4 (n = 2),20 which exhibit varying degrees of condensation among SnSe4 tetrahedra. Although Description
#!/bin/bash # testing the exit status var1=10 var2=30 var3=$[ $var1 + var2 ] exit $var3
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